HS
Huasheng Precision
Dongguan · Est. 2009
Case study / Medical

A PEEK enclosure —
validated through 50 autoclave cycles.

A German medical-device OEM needed the body of a reusable laparoscopic tool machined from PEEK. The part had to survive 50 cycles of 134 °C prevacuum steam sterilization without dimensional drift outside 0.1 mm. Here is what we did and what the post-cycle measurements showed.

The brief

Our customer is a German OEM that builds reusable laparoscopic tools under their own brand and private-label. The enclosure is the body of one of their tools — the surgeon’s hand grips it, the internal mechanism mounts to it, and six O-rings seal against machined faces inside the cavity. It is reusable, sterilized between patients by the hospital, and expected to survive at least 300 cycles over its service life before retirement.

Their previous vendor had held dimensional tolerances on first articles but the enclosures walked out of spec after 10 to 15 autoclave cycles — the bore went out-of-round and the O-ring seal failed. Our job was to requalify the part with documented 50-cycle stability as a floor.

Why the previous shop’s parts failed

We requested a used sample from the field and measured it on our CMM. What we saw was classic release of through-thickness residual stress: the sealing bore had ovalized by 0.12 mm after 12 cycles, and the long-axis length had shrunk 0.04 mm. The material was right, the geometry was right — the previous shop had skipped the pre-machining anneal on the plate and had taken finish passes too aggressively, leaving surface stress that released under the thermal cycling.

The lesson we wrote into our own medical-PEEK protocol after this job: anneal the plate, anneal again mid-process for parts with ribs or deep pockets, finish with at least 0.1 mm stock for light removal. It adds roughly 4 hours of oven time per lot. It is the difference between parts that pass validation and parts that come back after 15 cycles.

Process plan

Rough mill from 40 mm annealed plate in a single setup on a 3-axis vertical cell, leaving 0.5 mm of stock on all features. Remove from fixture, post-rough anneal at 150 °C for 1 hour in an air-circulating oven. Return to the cell, re-indicate datums, semi-finish to 0.15 mm stock, finish to final dimension with fresh tools and a light chip load. Final cleaning in isopropanol, visual inspection for any cosmetic defects, dimensional inspection on CMM. Pack in cleanroom-grade pouches.

The 50-cycle validation

The customer specified the validation cycle and we ran it through an accredited lab. Five parts entered the cycle at dimension Zero. We pulled them at cycle 1, 5, 10, 25, and 50 and CMM-measured the same twelve features each time. Bore diameter drifted 0.06 mm over 50 cycles, 0.04 mm of which happened in the first five cycles. All features stabilized by cycle 25. The customer’s acceptance criterion was 0.1 mm total — we passed with 40 % margin.

The lab report plus our CMM data and material cert became the supplier-qualification package. The customer’s regulatory team signed off four weeks later.

Ongoing production

We run 80 pieces per quarter on this part now, on a standing PO. Every lot ships with a DHR packet: material cert to the feedstock lot, CMM report on three parts, visual inspection record, cleaning record, and cleanroom packaging log. Unit price dropped 8 % between first article and third lot as we tuned the fixture and removed a redundant inspection step.

If you are building a reusable device and your current shop isn’t holding dimensional stability through sterilization cycles, send us the drawing plus the cycle spec. We will scope first-article, validation, and standing production and come back with a timeline inside a week.

/ FAQ

Frequently asked questions

Q01What is 450G and why that grade specifically?+
PEEK 450G is Victrex’s unfilled medical-grade resin. Unfilled means it machines cleanly without abrasive glass or carbon fibre wear on the tooling, which matters for a part with six O-ring sealing surfaces where you cannot have embedded hard particles. Filled PEEKs (30 % GF or CF) are stiffer and cheaper per kg, but the sealing performance degrades and the required surface finish is 3× harder to hold.
Q02How do you keep PEEK from warping during machining?+
PEEK’s glass transition is around 143 °C, well above room temperature, but it has internal residual stress from the plate’s extrusion. Our protocol: anneal the raw plate at 200 °C for 2 hours before any cutting (customer drew the blank from an already-annealed lot), keep machining temperatures under 120 °C by running dry with a strong air blast, and take multiple rough passes leaving at least 0.3 mm stock before a final light finish. On this job we also did an intermediate post-rough anneal at 150 °C for 1 hour, which reduces through-thickness stress and kept the sealing bore round to within 0.015 mm.
Q03How is the material certified for a reusable medical device?+
The customer specified material drawn from a lot with ISO 10993-5 in-vitro cytotoxicity clearance, which Victrex publishes per batch on their medical-grade line. We buy from Victrex’s authorized distributor in China, which supplies the original Victrex certificate of conformance, the ISO 10993-5 test report, and the lot traceability number with every shipment. That documentation is archived with the part’s DHR and shipped to the customer.
Q04What did the 50-cycle autoclave validation actually look like?+
We built five parts from the first production run, sent them to an ISO 17025 test lab in Shanghai, and ran a prevacuum steam cycle at 134 °C / 5 min plateau / 3 pre-pulses, following DIN EN ISO 17665. We measured all critical features on the CMM at cycle 0, 1, 5, 10, 25, and 50. Dimensional drift plateaued by cycle 25 — the first few cycles saw 0.04 mm of relaxation on the bore as residual stress released, then stable. The customer accepted the validation and added our shop as an approved supplier for the part.
Q05Can you do this on a one-off prototype?+
Yes — single-piece PEEK prototypes run about 7 days for a part of this size, no autoclave validation, no material-cert archive. If you want to evaluate geometry and fit before committing to validation, that is the right path and most of our medical customers start there. The step up to a validated production run costs roughly 3× the first-article price because of the material-cert archive and the multi-cycle inspection.
Q06What else do medical-device customers typically ask for?+
A DHR (device history record) packet per lot with inspection data and material cert. Cleanroom handling during final inspection and packaging — we have an ISO Class 8 room on-site. Passivation or cleaning procedures on non-PEEK components if they mate with this enclosure (stainless steel tools typically require passivation per ASTM A967). Batch-level traceability from raw stock to final crate. We’ve built all of these into the standard medical-job flow; call them out in the RFQ and you’ll see them line-itemed in the quote.
Start a project

Planning a reusable medical part in PEEK?

Tell us the sterilization cycle, the dimensional band you need to hold through it, and the target volume — we’ll scope first-article plus validation.